电子显微镜分析仪

Quantax Micro-XRF

Trace Element Sensitivity with Minimal Sample Preparation

High-Speed Elemental X-ray Mapping even over Large Areas

Film Thickness Analysis

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Highlights

10 ppm
检测极限
Enabling trace element analysis due to the lower spectral background
4 mm/s
travel speed
The optional Rapid Stage enables high-speed mapping over large areas
1 nm -40 µm
layer thickness range
Thin films starting from 1 nm up to multiple layer structures of 40 µm can be analyzed

Micro-XRF作为SEM中EDS分析的免费分析技术

  • Micro-X射线荧光(Micro-XRF)光谱分析是使用扫描电子显微镜(SEM)对传统能量色散光谱(EDS)分析进行互补的非破坏性分析技术。此类分析对于表征未知样品中元素组成的表征至关重要,范围从大厘米大小的不均匀标本到小千分尺颗粒。
  • X射线激发对痕量元素检测产生更高的灵敏度(低至低至10 ppmfor certain elements), an extended X-ray spectral range (最多40 keV),以及样本中更深度的信息。
  • Equipped with an X-ray tube in combination with a micro-focusing X-ray optic yields small spot sizes of30 µm高强度吞吐量。
  • 一个模块化压电阶段,专门设计用于安装在现有SEM阶段顶部4毫米/秒. This enables the acquisition of X-ray mapping data over a sample size of 50 x 50 mm (or higher), incorporating light element spectral data as well as trace element and/ or higher energy X-ray data in a fast and user-friendly workflow.
  • The larger depth of X-ray excitation allows the characterization of multilayer systems starting from1 nm and ranging up to 40 µm, which is not possible with electron excitation.

Benefits

Expand your SEM analytical capabilities with the Micro-XRF and Rapid Stage

  • Dual beam potential, both an e-beam and an X-ray beam, which offers new possibilities for the material characterization - Investigate samples simultaneously with both sources.
  • 使用同一检测器同时进行电子束/微XRF采集,并包含光元素光谱数据以及痕量元素和/或更高的能量X射线数据。
  • Both XTrace andRapid Stageare seamlessly integrated in theESPRIT软件.
  • 通过将电子激发的更好光元灵敏度与XRF的更好的痕量元素灵敏度相结合,将EDS和Micro-XRF定量结合起来,从而实现了更完整的样品表征。
  • Simultaneous mapping with micro-XRF and e-beam excitation, combining the advantages from both worlds. Exciting the light elements (carbon to sodium) using the e-beam and heavier elements by micro-XRF.
  • Separate peaks & extended spectral range enables the capability to see the high energy K- lines since they are less complex and less overlapped.
  • Minimum sample prep – no conductive sample surface and no extensive polishing required
  • 无标准和基于标准的量化。

申请

Incorporating Light and Heavy Elements even at Low Concentration Levels at a µm Scale

异国情调的铜样本El Tesoro我在智利。

矿物学样品的大面积映射

新的快速阶段专门为SEMS设计,以使大面积映射通过毫米(mm)到厘米(cm)尺度。这将消除潜在的SEM X射线强度变化与低放大映射相关的伪像,从而在以前无法实现的时代庄园中增强元素和矿物学信息。
守护神ge area map of an exotic Cu deposit sample.

外来CU沉积中的元素和矿物质分布

The ability to observe elemental changes within samples is important to understand geological processes and ore deposit genesis. The dual source system which incorporates a micro-XRF on a SEM enables elemental X-ray mapping over large areas, which shows major, minor and also trace elements on the ppm scale.
样品来自新西兰的Karangahake金矿。

Dual Source Applications for Exploration and Mining: Au-bearing Epithermal Samples

Micro-XRF与SEM的组合可以使从厘米(CM)到毫米(mm)到微米(µM)及以下单独系统中的多个尺度分析样品。因此,通过将Micro-XRF添加到SEM中,您可以将SEM转换为双源系统,这意味着有2个激发源,即电子束和光子光束。可以单独或同时使用源来生成将使用相同EDS检测器测量的样品X射线。
守护神ge area map of a diamond-bearing eclogite.

Mantle Petrology and the Source of Diamonds

我们提供了来自含钻石的纽兰兹金伯利岩(南非,卡普瓦尔·克拉顿)的地幔石榴石状皮橄榄石的SEM-XRF元素图。各个元素的强度表明样品中存在的某些矿物质。
守护神ge area maps of soil samples.

Identification of Contaminants and Toxins in Soils

守护神ge Area Mapping (Hypermaps) using SEM-XRF can be performed on samples with topography. That is, minimal sample preparation is required and the sample can be analyzed directly without any degredation. This is particularly relevant in the analysis of soils, where any form of sample preparation, such as mounting and polishing or carbon coating, may alter the specimen.
CIGS structure

Thin Film Analysis with SEM micro-XRF

随着X射线可能通过物质,X射线荧光(XRF)允许确定层厚度。使用SEM上的Micro-XRF,通过在千分尺尺度上的空间分辨率使层分析(厚度和组成)可行。层分析强烈基于使用原子基本参数(FP)的定量。

配件

Rapid Stage

快速阶段可以安装在SEM阶段的顶部,以在大型样品区域快速映射。