小角度X射线散射(SAXS)

NANOSTAR

Your telescope to the Nano-universe | Dedicated Small Angle X-Ray Scattering (SAXS) with modular design for experimental flexibility

NANOGRAPHY - SAXS - WAXS - GISAXS

Herostananostar-metaljet

强调

Ø14厘米
large 2D active area with the VÅNTEC-500
The large full field of view collects the whole scattering signal, isotropic or anisotropic, in a single shot.
> 200 nm
accessible length scale
模块化设计允许大量散射覆盖范围,以使纳米结构完全表征大于125 nm的长度尺度。
5-150 cm
sample to detector distance
Wide range of detector positioning to optimize the scattering coverage to the sample.
带有延长次级梁路径的纳米托尔

The NANOSTAR with its incomparable modularity is the ideal tool for characterization of nanostructures and nanostructured surfaces by Small-Angle X-Ray Scattering (SAXS), Grazing-Incidence Small-Angle X-ray Scattering (GI-SAXS), Wide-Angle X-Ray Scattering (WAXS), and Nanography. The mirror-conditioned pinhole collimation system produces a parallel, ideal circular beam shape with high intensity and low parasitic scatter. The extra-large (XL) sample chamber accommodates a variety of dedicated and 3rd party sample stages for measurements of many sample types under all conditions. Finally the scattered signal is collected with a large, low background, highly sensitive 2D detector for isotropic and anisotropic samples.

特征s

NANOSTAR Features

IµS微焦点源

这种独特的X射线源可提供非常稳定和强烈的斑点X射线梁,而无需进行水冷却。得益于其强大的设计,该消息来源具有3年的保修。IµS包括集成的MONTEL,最先进的2-D光束成型光学元件,以最高强度。这种并排的多层镜设计可从源捕获大的X射线固体角度,并在高度平行和单色梁中有效地重定向。

NANOSTAR Features

XL样品室

这个方便的超大(XL)样品室配备了许多额外的直通端口,可以在真空,惰性气体或大气条件下进行操作。它可以容纳许多其他标准组件,用于个性化处理多个样本以及第三方和定制阶段,以最大程度的可见性。一个具有较大翻译范围和次级电动参考样品架的机动X-y阶段,使自动样品对齐和参考和背景扫描快照!

NANOSTAR Features

VÅNTEC-500 2D detector

The VANTEC-500 2-D detector with MikrogapTM理想的技术满足所有需求of a dedicated SAXS system. First, no need for gas, water, or routine maintenance and no concerns for intense radiation or movement damage results in detector that is robust and very easy to use. A large active area (14 cm diameter) to enable huge angular coverage with full field of view. Incredibly low background and high maximum count rate for fantastic dynamic range and sensitivity to weakly scattering samples. Excellent spatial resolution to resolve closely spaced scattering features. No other detector can offer these combination of ideal features for these applications.

Applications

Key Applications

纳米级应用

Small-Angle and Wide-Angle X-Ray Scattering (SAXS & WAXS)

小角度X射线散射(SAXS)是由嵌入不同电子密度基质中的颗粒引起的现象。如果粒径范围从1 nm到200 nm,则散射角位于0°至5°的范围内,具体取决于所使用的X射线波长。颗粒越小,较宽的是散射角。

Any arrangement of particles in any medium shows a difference in electron density, which results in a specific pattern when executing a SAXS experiment. Along with the size of the particles, SAXS can also determine their shape, their distance apart and size distribution from the 2-D pattern. Particles can be dissolved macromolecules, precipitations in metals, mineral particles in biological tissues, and surfactant micelles.

In contrast to SAXS, Wide Angle X-ray Scattering (WAXS) examines structures on the Angstrom level, which are typically interplanar distances of crystalline structures. Often WAXS is used to analyze Bragg the X-ray diffraction (XRD) pattern which can help determine crystalline structure, degree of crystallinity, crystallite size, and phase composition (Phase ID). WAXS data can be collected at the same time (simultaneously) as SAXS data with a 2nd detector positioned much closer to the sample.

纳米级应用

Grazing-Incidence SAXS (GI-SAXS)

为了探测表面和地下结构细节,样品以放牧的入射率几何形状进行测量。入射角接近所谓的总反射的临界角,通常位于0.1至0.7度之间。在放牧的小角度X射线散射(GISAXS)实验中,通过二维检测器通过二-D检测器在非旋转方向上收集扩散的散射强度。

A dedicated GI-SAXS stage with motorized tilt is used to align the sample in the beam.

纳米级应用

Nanography

A Nanography investigation utilizes the motor-driven XY stage integrated into the sample chamber of the NANOSTAR. This allows a selected region of the sample to be scanned through the X-ray beam automatically. The intensity distribution (or other scattering parameter) can then be displayed by means of a color-coded contour plot.

Nanography permits fast and selective detection of relevant measuring points with inhomogeneous samples and allows even small samples to be positioned precisely. Each individual point of the complete Nanography image itself represents the integral SAXS/WAXS intensity collected by the 2-D.

规格

NANOSTAR Specifications

特征

规格

Benefit

IµS微焦点源

Air-cooled, high intensity, micro-focus X-Ray source

低功率使用(30W)

3 year standard warranty

No need for water chiller

高功率密度导致强度增加

Integrated Montel mirrors for ideal beam conditioning

Scatex针孔

理想的圆形光束形状具有可忽略的寄生背景散射。

没有寄生孔边缘散射

Higher resolution / Higher flux

更紧凑的准直梁路径允许更长的探测器距离

Easy, stable, pinhole alignment

XL样品室

超大型腔室,带有电动XY阶段,可用于样品定位,映射和多功能标准和第三方阶段。

Inner dimensions: 287 mm x 501 mm x 380 mm (W x H x D)

额外供应连接的法兰

XY阶段,具有80 mm x 130毫米翻译

Motorized reference sample wheel

在真空,空气或惰性气气中操作

VÅNTEC-500 2D detector

较大的活动区域,低背景,高灵敏度2D检测器

Large active area (14 cm diameter) for full frame of view SAXS/WAXS scattering images

Very low background for highest sensitivity

Excellent spatial resolution (68 micron pixel size)

无维护(无需水/空气或对偏置下强的原代光束或探测器运动的敏感性)

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