X射线衍射(XRD)

D8 ADVANCE Plus

Taking the D8 ADVANCE beyond powder.
Herostaged8Advance

Highlights

The D8 ADVANCE Plus: Multipurpose Materials Research

>1x10β光子/s
eiger2 r 500k的计数速率能力
Eiger2 R 500K拥有最大的动态范围,可实现无吸收器的测量,并具有一致的信号到噪声。
3x2
TWIN and TRIO optics
Fully automatic switching between up to 6 different beam geometries
4
Centric axes
The Compact Cradle Plus transforms the D8 ADVANCE from a 2 to 4 axis diffractometer with the addition of Phi and Psi.
布鲁克’s unique alignment guarantee
Learn more

D8 ADVANCE Plus - maximum flexibility meets unparalleled ease-of-use

The D8 ADVANCE Plus is a D8 ADVANCE variant representing the ultimate X-ray platform for multi-purpose, multi-user laboratories. The system perfectly matches the needs of all sample types including powders, bulk materials, fibers, sheets and thin-films (amorphous, polycrystalline and epitaxial):

  • traditional X-ray powder diffraction (XRD)
  • Pair Distribution Function (PDF)analysis
  • Small and Wide Angle X-ray Scattering (SAXS, WAXS)
  • XRR (reflectometry) and HRXRD (rocking curves, reciprocal space mapping)
    在环境和非事实条件下。

The real beauty of the system is its ability to switch between up to 6 different beam geometries, from focusing Bragg-Brentano geometry for powders to high-resolution parallel-beam Kα1 geometry for epitaxial thin films and everything in-between. Fully software controlled, at the push of a button.

无论样品类型和应用程序,和no matter if you are a novice or an expert user: The D8 ADVANCE Plus sets a new benchmark in data quality thanks to its unparalleled flexibility and easy-of-use.

Features

Key Features

D8 Advance Plus功能

三重奏光学

The patented TRIO optics simplify the usage of the D8 ADVANCE, allowing the largest variety of applications and sample types. With user convenience in mind, the system features automatic, motorized switching between up to 6 different beam geometries. Without manual user intervention, the system is capable of switching between three beampaths:

  • Focusing Bragg-Brentano for powders
  • 毛细管,GID和XRR的高强度平行梁Kα1,2
  • 外延薄膜的高分辨率平行梁Kα1几何形状

It is perfectly suited for all sample types including powder, bulk, fiber, sheet and thin-film (amorphous, polycrystalline and epitaxial) under ambient or non-ambient conditions.

D8 Advance Plus功能

bob综合游戏材料研究阶段

The Compact UMC and Compact Cradle Plus extend the sample handling capability of the D8 ADVANCE Plus allowing complex precision motion of the sample. The Comact UMC stage features motorized motion of 25 mm in X, 70 mm in Y and 52 mm in Z with 2 kg sample capacity for analysis of large bulk samples or multiple smaller samples. The Compact Cradle Plus includes unlimited Phi rotation and Psi tilt from -5° to 95° for stress, texture and epitaxial thin film analysis. In addition, the Compact Cradle Plus features a vacuum utility feedthrough allowing samples to be held in place with either a small thin film sample holder or large manual XY table. Both stages accommodate dome temperature stages for non-ambient analysis. They also utilize the DIFFRAC.DAVINCI stage bayonet mounting system for easy exchange of the sample stage.

D8 Advance Plus功能

eiger2 r探测器

Multimode functionality (0D-1D-2D, snapshot and scanning modes) allows the EIGER2 R detectors to cover a wide range of measurement methods ranging from powder to materials research applications. Not the typical jack of all trades, the EIGER2 is a master of all applications. With a dynamic range that allows absorber free measurements, large 1D size for ultra fast powder measurements and rapid reciprocal space maps and over 500k pixels for large two dimensional coverage, the EIGER2 sets a new standard for multimode detectors. The EIGER2 combines beamline detector technology from DECTRIS Ltd. with software and hardware integration from BRUKER into a seamless easy to use solution.

Applications

One Diffractometer - All Applications

D8 Advance Plus申请

Powder Diffraction

X射线粉末衍射(XRPD)技术是材料表征的最重要工具之一。bob综合游戏嵌入到粉末图案中的许多信息直接从存在的相的原子排列中得出。D8 Advance和Fiffrac.Suite软件允许支持简单执行常见XRPD方法:

  • Identification of both crystalline and amorphous phases and determination of specimen purity
  • 定量分析的水晶和埃莫phous phases in multi-phase mixtures
  • Microstructure analysis (crystallite size, microstrain, disorder…)
  • Bulk residual stress resulting from thermal treatment or machining in manufactured components
  • Texture (preferred orientation) analysis
  • 索引,Ab-Initio晶体结构测定和晶体结构的细化
D8 Advance Plus申请

残余压力和质地分析

剩余的应力和质地测量通常是在将材料推到极限的工业金属样品上。bob娱乐平台bob综合游戏通过缓解拉伸应力或在样品表面诱导压力应力,可以大大延长其功能寿命。这可以通过热治疗或物理过程(例如shot peing)来完成。构成大量样品的微晶的方向决定了裂缝传播的方式。通过在材料中形成特定的纹理,可以大大提高其特性。这两种技术在优化较前沿制造方法(例如添加剂制造)方面也很重要。

D8 Advance Plus申请

薄膜和涂料

Analysis of thin films and coatings is based on the same principles of XRPD, but with further beam conditioning and angular control. Typical examples include, but are not limited to, phase identification, crystalline quality, residual stress, texture analysis, thickness determination and composition vs strain analysis. Analysis of thin films and coatings is focusing on properties of layered materials with nm to µm thickness, ranging from amorphous and poly-crystalline coatings to epitaxially grown films. The D8 ADVANCE and the DIFFRAC.SUITE software enable high quality analyses of thin films including:

  • Grazing Incidence Diffraction
  • X-Ray Reflectometry
  • High Resolution X-ray Diffraction
  • 相互空间映射

规格s

D8 ADVANCE Plus Specifications

Feature

规格

益处

三重奏光学

软件push-button switch between:

Motorized Divergence Slit (Bragg-Brentano)

高强度KA1,2平行梁

High Resolution Ka1 Parallel Beam

Patents: US10429326, US6665372, US7983389

全自动,电动的切换在多达6个不同的光束几何之间,而无需任何手动用户干预

非常适合所有样品类型,包括粉末,散装材料,纤维,床单和薄膜(无定形,多晶和外延)bob综合游戏

LYNXEYE XE-T

Energy Resolution: < 380 eV @ 8 KeV

检测模式:0D,1D,2D

Wavelengths: Cr, Co, Cu, Mo and Ag

专利:EP1647840,EP1510811,US20200033275

不需要Kß滤波器和次级单色器

用Cu辐射对Fe-Fluorescense的100%过滤

比传统探测器系统快450倍

BRAGG2D: Collect 2D data with a divergent primary line beam

Unique detector warranty: No defective channels at delivery time

eiger2 r

最新一代的多模式(0D/1D/2D)检测器基于Dectris Ltd开发的混合光子计数技术。

Seamless integration of 0D, 1D and 2D detection in step, continuous and advanced scanning modes

Ergonomic, alignment-free detector rotation to optimize γ or 2Θ angular coverage

使用完整的探测器视野

连续可变的检测器定位以平衡角度覆盖范围和分辨率

TWIST.TUBE

Easy, fast, and alignment-free switch between line and point focus applications

没有电缆或水管的断开连接或管子的卸载

Davinci.Design:焦点方向的完全自动检测和配置

Compact UMC Stage

电动X:25毫米

机动Y:70毫米

Motorized Z: 52 mm

Capacity: 2 kg

梁中大样本感兴趣区域的精确定位

Mounting multiple samples for automatic measurements

Compact Cradle Plus

Motorized Phi: Unlimited

Motorized Psi: -5° to 95°

Vacuum utility feedthrough for worry-free sample mounting

Full 4 axis diffraction allows texture, residual stress and thin film measurements

D8 GONIOMETER

带有独立步进电动机和光学编码器的两圈圆锥体计

布鲁克(Bruker)独特的对齐保证表现出无与伦比的准确性和精确度

Absolutely maintenance free drive mechanism / gearings with lifetime lubrication

非ambient

温度:从〜85k到〜2500K不等

压力:10-⁴MBAR最多10 bar

湿度:5%至95%RH

Investigations under ambient and non-ambient conditions

轻松地与diffrac.davinci交换阶段

配件

XRD Components

XRD Components

布鲁克XRD solutions consist of high performance components configured to meet the analytical requirements. The modular design is the key to configure the best instrumentation.

All categories of components are part of Bruker’s key competence, developed and manufactured by Bruker AXS, or in close cooperation with third party vendors.

布鲁克XRD components are available for upgrading the installed X-ray systems for improving their performance.

软件

PLAN.MEASURE.ANALYZE with DIFFRAC.SUITE

DIFFRAC.SUITE Software

Diffrac.Suite™提供了各种软件模块,可用于X射线粉末衍射数据采集和评估。根据Microsoft的.NET技术,fiffrac.Suite提供了现代软件技术的所有优势,可稳定,最大程度的使用和网络。

完全可定制的用户界面的特征是插入式框架,提供了共同的外观,感觉和操作。所有测量和评估软件模块都可以作为单个应用程序操作,也可以将其集成到diffrac.suite的插件框架中。无限网络允许在客户网络中访问和控制任意数量的D2 Phaser,D8 Advance,D8 Discover和D8 Endeavor衍射仪。

Measurement Software:
向导– Method planning
指挥官– Method execution and direct measurements
工具 - 服务接bob电竞官方网站口
Powder Diffraction Software:
dquant– Quantitative phase analysis
伊娃– Phase identification and quantitative phase analysis
TOPAS- 概况分析,定量分析,结构分析

Materials Research Software:
萨克斯- 小角度X射线散射软件
XRR– Comprehensive X-ray reflectometry analysis
TEXTURE- 全方位纹理分析满足易用性
LEPTOS- 薄膜分析/残留应力调查

网络研讨会

Support

Service & Support

We provide:

  • Help desk support from highly-skilled troubleshooting professionals, to isolate and resolve hard- and software problems
  • 基于Web的远程仪器服务用于服务诊断和应用程序支持bob电竞官方网站
  • Merged reality support – a virtual engineer at your side (video)
  • 根据您的要求,计划维护
  • 客户现场维修和维护服务bob电竞官方网站
  • 备件的可用性通常在全球的几个工作日或几个工作日之内
  • Compliance services for installation qualification, operational qualification / performance verification
  • Site planning and relocation
  • Find your nexttraining course

看看我们支持网站for:

  • 软件更新
  • 产品手册和安装指南
  • Training videos

Registration required.